Home / Articles / Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy

Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy

Vadim V Kachala 1
Vadim V Kachala
, 
Levon L'vovich Khemchyan 1
Levon L'vovich Khemchyan
, 
Aleksey Sergeevich Kashin 1
Aleksey Sergeevich Kashin
, 
Nikolay Vladimirovich Orlov 1
Nikolay Vladimirovich Orlov
, 
Alexey Aleksandrovich Grachev 1
Alexey Aleksandrovich Grachev
, 
Sergey Sergeyevich Zalesskiy 1
Sergey Sergeyevich Zalesskiy
, 
1 N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Published 30 November 2012
Communication , Volume 82, Issue 7, 648-685
255
Share
Cite this
GOST
 | 
Cite this
GOST
Kachala V. V. et al. Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy // Russian Chemical Reviews. 2013. Vol. 82. No. 7. pp. 648-685.
GOST all authors (up to 50)
Kachala V. V., Khemchyan L. L., Kashin A. S., Orlov N. V., Grachev A. A., Zalesskiy S. S., Ananikov V. P. Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy // Russian Chemical Reviews. 2013. Vol. 82. No. 7. pp. 648-685.
RIS
 | 
Cite this
RIS
TY - JOUR
DO - 10.1070/RC2013v082n07ABEH004413
UR - https://rcr.colab.ws/publications/10.1070/RC2013v082n07ABEH004413
TI - Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy
T2 - Russian Chemical Reviews
AU - Kachala, Vadim V
AU - Khemchyan, Levon L'vovich
AU - Kashin, Aleksey Sergeevich
AU - Orlov, Nikolay Vladimirovich
AU - Grachev, Alexey Aleksandrovich
AU - Zalesskiy, Sergey Sergeyevich
AU - Ananikov, Valentin Pavlovich
PY - 2013
DA - 2012/11/30
PB - ANO Editorial Board of the journal Uspekhi Khimii
SP - 648-685
IS - 7
VL - 82
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors)
@article{2013_Kachala,
author = {Vadim V Kachala and Levon L'vovich Khemchyan and Aleksey Sergeevich Kashin and Nikolay Vladimirovich Orlov and Alexey Aleksandrovich Grachev and Sergey Sergeyevich Zalesskiy and Valentin Pavlovich Ananikov},
title = {Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy},
journal = {Russian Chemical Reviews},
year = {2013},
volume = {82},
publisher = {ANO Editorial Board of the journal Uspekhi Khimii},
month = {Nov},
url = {https://rcr.colab.ws/publications/10.1070/RC2013v082n07ABEH004413},
number = {7},
pages = {648--685},
doi = {10.1070/RC2013v082n07ABEH004413}
}
MLA
Cite this
MLA
Kachala, Vadim V., et al. “Target-oriented analysis of gaseous, liquid, and solid chemical systems with mass spectrometry, nuclear magnetic resonance spectroscopy, and electron microscopy.” Russian Chemical Reviews, vol. 82, no. 7, Nov. 2013, pp. 648-685. https://rcr.colab.ws/publications/10.1070/RC2013v082n07ABEH004413.
Views / Visits / Downloads
17 / 17 / 3

Abstract

In the present review we describe emerging tendency for creating target-oriented analytical approach designed to solve important chemical tasks by using a combination of analytical tools. The concept is illustrated by selected examples of advances of NMR spectroscopy, mass spectrometry and electron microscopy in the studies of gas-phase, liquid-state and solid-state chemical systems. Comparative description of chemical applications of these analytical methods is presented and discussed.

Bibliography --- 359 references.

References

1.
1
A. A. Krasnovskii
Dokl. Akad. Nauk SSSR , 1948
3.
A High Intensity Mass-Spectrometer
Smythe W.R., Rumbaugh L.H., West S.S.
Physical Review A , 1934
4.
Californium-252 Plasma Desorption Mass Spectroscopy
Macfarlane R.D., Torgerson D.F.
Science , 1976
5.
Mass Spectral Correlations
Photochemistry and Radiation Chemistry , 1982
6.
6
V. B. Evstigneev
Dokl. Akad. Nauk SSSR , 1953
7.
7
E. Rabinowitch
"Photosynthesis" , 1956
8.
Electrospray ionization for mass spectrometry of large biomolecules
Fenn J.B., Mann M., Meng C.K., Wong S.F., Whitehouse C.M.
Science , 1989
9.
9
V. H. Lynch
Carnegie Inst. Year Book , 1954
10.
10
T. A. Kryukova
"Polyaro-graficheskii Analiz" (Polarographic Analysis) , 1959
11.
11
T. T. Bannister
Diss. Abstr. , 1959
14.
14
V. B. Evstigneev
Zhur. Fiz. Khim. , 1958
15.
15
A. S. Holt
"Research in Photosynthesis" , 1957
18.
Unusual control of reaction selectivity through a subtle change in the ligand: Proof of concept and application in Pd-catalyzed C-P bond formation
19.
10.1002/1521-3773(20020902)41:17<3096::AID-ANIE3096>3.0.CO;2-X
21.
Comprehensive multiphase NMR spectroscopy: Basic experimental approaches to differentiate phases in heterogeneous samples
Courtier-Murias D., Farooq H., Masoom H., Botana A., Soong R., Longstaffe J.G., Simpson M.J., Maas W.E., Fey M., Andrew B., Struppe J., Hutchins H., Krishnamurthy S., Kumar R., Monette M., et. al.
Journal of Magnetic Resonance , 2012
22.
22
A. A. Krasnovskii
Dokl. Akad. Nauk SSSR , 1958
23.
Gas-Phase NMR Spectroscopy
SUAREZ C.
The Chemical Educator , 1998
24.
Gas-phase NMR spectroscopy
Jameson C.J.
Chemical Reviews , 1991
25.
15N NMR Spectroscopy in Structural Analysis
Marek R., Lycka A.
Current Organic Chemistry , 2002
26.
Facile structural elucidation of imidazoles and oxazoles based on NMR spectroscopy and quantum mechanical calculations
28.
28
A. A. Krasnovskii
Dokl. Akad. Nauk SSSR , 1955
29.
Goldstein J.I., Newbury D.E., Echlin P., Joy D.C., Lyman C.E., Lifshin E., Sawyer L., Michael J.R.
2003
30.
30
V. B. Evstigneev
Dokl. Akad. Nauk SSSR , 1954
32.
Autocatalytic gas-phase dehydrogenation of ethane
Snytnikov V.N., Mishchenko T.I., Snytnikov V.N., Malykhin S.E., Avdeev V.I., Parmon V.N.
Research on Chemical Intermediates , 2011
34.
Microwaves in Heterogeneous Gas‐Phase Catalysis: Experimental and Numerical Approaches
Durka T., Van Gerven T., Stankiewicz A.
Chemical Engineering and Technology , 2009
35.
Gas-phase oxypyrolysis of light alkanes
Arutyunov V.S., Magomedov R.N.
Russian Chemical Reviews , 2012
36.
Gas phase chemistry of neutral metal clusters: Distribution, reactivity and catalysis
Yin S., Bernstein E.R.
International Journal of Mass Spectrometry , 2012
37.
Gas-phase propene epoxidation over coinage metal catalysts
Huang J., Haruta M.
Research on Chemical Intermediates , 2011
43.
43
N. Bunge
Ber. Deutsch. Chem. Ges. , 1870
44.
Selective Activation of Alkanes by Gas-Phase Metal Ions
Roithová J., Schröder D.
Chemical Reviews , 2009
45.
Gas-phase ion chemistry in organometallic systems
Operti L., Rabezzana R.
Mass Spectrometry Reviews , 2006
46.
Hydrated metal ions in the gas phase
Beyer M.K.
Mass Spectrometry Reviews , 2007
47.
Relativistic Effects in Gas-Phase Ion Chemistry: An Experimentalist's View
48.
Gas-phase enantioselective reactions in noncovalent ion-molecule complexes
Speranza M., Gasparrini F., Botta B., Villani C., Subissati D., Fraschetti C., Subrizi F.
Chirality , 2009
50.
Gas-phase polar cycloadditions
Eberlin M.N.
International Journal of Mass Spectrometry , 2004
52.
10.1002/1099-1395(200102)14:2<109::AID-POC344>3.0.CO;2-J
55.
Gas-phase radical chemistry in the troposphere
Monks P.S.
Chemical Society Reviews , 2005
56.
Laboratory Astrochemistry: Gas-Phase Processes
Smith I.W.
Annual Review of Astronomy and Astrophysics , 2011
59.
A Comparative Study of Homolytic Reactions of Fullerenes with Aldehydes in a Mass Spectrometer under Electron Impact and in Solution under UV Irradiation
Lyakhovetsky Y.I., Pleshkova A.P., Shilova E.A., Ponomareva T.V., Gasanov R.G., Tumanskii B.L., Borisov Y.A., Nekrasov Y.S.
European Journal of Mass Spectrometry , 2012
60.
Electron ionization mass spectra and tautomerism of substituted 2-phenacylquinolines
Martiskainen O., Gawinecki R., Ośmiałowski B., Wiinamäki K., Pihlaja K.
Rapid Communications in Mass Spectrometry , 2009
61.
Aromatic Hydroxylation of Indan by o -Xylene-Degrading Rhodococcus sp. Strain DK17
Kim D., Lee C.H., Choi J.N., Choi K.Y., Zylstra G.J., Kim E.
Applied and Environmental Microbiology , 2010
63.
Oxidation Mechanisms of CF2Br2 and CH2Br2 Induced by Air Nonthermal Plasma
Schiorlin M., Marotta E., Dal Molin M., Paradisi C.
Environmental Science & Technology , 2012
64.
Simple Coupling of Gas Chromatography to Electrospray Ionization Mass Spectrometry
Brenner N., Haapala M., Vuorensola K., Kostiainen R.
Analytical Chemistry , 2008
67.
Mass spectrometry with photoionization of N-alkanes, alcohols, ketones, esters, and amines at atmospheric pressure
Revel'skii I.A., Yashin Y.S., Voznesenskii V.N., Kurochkin V.K., Kostyanovskii R.C.
Russian Chemical Bulletin , 1986
68.
68
N. N. Mel'nikov
Zhur. Obshch. Khim. , 1946
69.
Microchip for Combining Gas Chromatography or Capillary Liquid Chromatography with Atmospheric Pressure Photoionization-Mass Spectrometry
Haapala M., Luosujärvi L., Saarela V., Kotiaho T., Ketola R.A., Franssila S., Kostiainen R.
Analytical Chemistry , 2007
73.
Measurement and optimization of organic chemical reaction yields by GC–MS with supersonic molecular beams
Amirav A., Gordin A., Hagooly Y., Rozen S., Belgorodsky B., Seemann B., Marom H., Gozin M., Fialkov A.B.
Tetrahedron , 2012
74.
Detailed mass spectrometric and modeling study of isomeric butene flames
Schenk M., Leon L., Moshammer K., Oßwald P., Zeuch T., Seidel L., Mauss F., Kohse-Höinghaus K.
Combustion and Flame , 2013
75.
Combustion of butanol isomers – A detailed molecular beam mass spectrometry investigation of their flame chemistry
Oßwald P., Güldenberg H., Kohse-Höinghaus K., Yang B., Yuan T., Qi F.
Combustion and Flame , 2011
76.
Combustion chemistry and fuel-nitrogen conversion in a laminar premixed flame of morpholine as a model biofuel
77.
The Oxidative Mechanism in Electrophilic CH Activation: The Case of CH2F2and CH2Cl2
de Petris G., Rosi M., Ursini O., Troiani A.
Chemistry - An Asian Journal , 2013
79.
De novo analysis of electron impact mass spectra using fragmentation trees
Hufsky F., Rempt M., Rasche F., Pohnert G., Böcker S.
Analytica Chimica Acta , 2012
81.
Online Characterization of Particles and Gases with an Ambient Electrospray Ionization Source
Horan A.J., Gao Y., Hall W.A., Johnston M.V.
Analytical Chemistry , 2012
82.
Ambient ionization mass spectrometry: A tutorial
Huang M., Cheng S., Cho Y., Shiea J.
Analytica Chimica Acta , 2011
83.
An instrumentation perspective on reaction monitoring by ambient mass spectrometry
Ma X., Zhang S., Zhang X.
TrAC - Trends in Analytical Chemistry , 2012
84.
Mass Spectrometry: Recent Advances in Direct Open Air Surface Sampling/Ionization
Monge M.E., Harris G.A., Dwivedi P., Fernández F.M.
Chemical Reviews , 2013
85.
Protein and polymer analyses up tom/z 100 000 by laser ionization time-of-flight mass spectrometry
Tanaka K., Waki H., Ido Y., Akita S., Yoshida Y., Yoshida T., Matsuo T.
Rapid Communications in Mass Spectrometry , 1988
86.
86
V. B. Evstigneev
Dokl. Akad. Nauk SSSR , 1958
87.
87
J. F. Arens
"Advances in Organic Chemistry" , 1960
89.
A Mechanism for Ionization of Nonvolatile Compounds in Mass Spectrometry: Considerations from MALDI and Inlet Ionization
Trimpin S., Wang B., Inutan E.D., Li J., Lietz C.B., Harron A., Pagnotti V.S., Sardelis D., McEwen C.N.
Journal of the American Society for Mass Spectrometry , 2012
93.
Synthesis and crossover reaction of TEMPO containing block copolymer via ROMP
Adekunle O., Tanner S., Binder W.H.
Beilstein Journal of Organic Chemistry , 2010
94.
Monitoring Block-Copolymer Crossover-Chemistry in ROMP: Catalyst Evaluation via Mass-Spectrometry (MALDI)
Binder W.H., Pulamagatta B., Kir O., Kurzhals S., Barqawi H., Tanner S.
Macromolecules , 2009
97.
MALDI Mass Analysis of 11 kDa Gold Clusters Protected by Octadecanethiolate Ligands
Tsunoyama R., Tsunoyama H., Pannopard P., Limtrakul J., Tsukuda T.
Journal of Physical Chemistry C , 2010
100.
Carbon-Carbon Bond Activation in Saturated Hydrocarbons by Field-Assisted Nitrogen Fixation
Li G., Li X., Ouyang Z., Cooks R.G.
Angewandte Chemie - International Edition , 2012
101.
Absolute shielding scale for 31P from gas-phase NMR studies
Jameson C.J., De Dios A., Keith Jameson A.
Chemical Physics Letters , 1990
102.
Indirect spin–spin coupling constants in CH4, SiH4 and GeH4 – Gas-phase NMR experiment and ab initio calculations
103.
Multinuclear NMR spectroscopy in the gas phase
Jackowski K.
Journal of Molecular Structure , 2006
105.
NMR spectroscopy of cyclohexane. Gas-phase conformational kinetics
Ross B.D., True N.S.
Journal of the American Chemical Society , 1983
106.
Gas-Phase Dynamic NMR Study of the Internal Rotation in N-Trifluoroacetylpyrrolidine
Suarez C., Nicholas E.J., Bowman M.R.
Journal of Physical Chemistry A , 2003
108.
NMR study of stable radicals in the gas phase
Obynochny A.A., Maryasov A.G., Shakirov M.M., Grigoriev I.A.
Chemical Physics , 1993
110.
Hydrogenation of Fluoroolefins Studied by Gas Phase NMR:  A New Technique for Heterogeneous Catalysis
Kating P.M., Krusic P.J., Roe D.C., Smart B.E.
Journal of the American Chemical Society , 1996
111.
Bimolecular Kinetic Studies with High-Temperature Gas-Phase 19F NMR:  Cycloaddition Reactions of Fluoroolefins
Shtarov A.B., Krusic P.J., Smart B.E., Dolbier W.R.
Journal of the American Chemical Society , 2001
112.
Gas-Phase NMR Study of the DCl-HBr Isotope Exchange Reaction
Nibler J.W., Minarik P., Fitts W., Kohnert R.
Journal of Chemical Education , 1996
113.
Two-dimensional NMR correlation experiments in the gas phase
116.
Bimetallic Catalysis using Transition and Group 11 Metals: An Emerging Tool for CC Coupling and Other Reactions
117.
10.1002/1521-3773(20020104)41:1<26::AID-ANIE26>3.0.CO;2-9
118.
Formation of Carbon−Carbon Bonds under Catalysis by Transition-Metal Nanoparticles
Moreno-Mañas M., Pleixats R.
Accounts of Chemical Research , 2003
120.
N-Heterocyclic Carbenes in Late Transition Metal Catalysis
Díez-González S., Marion N., Nolan S.P.
Chemical Reviews , 2009
123.
(Thio)urea organocatalysis--what can be learnt from anion recognition?
Zhang Z., Schreiner P.R.
Chemical Society Reviews , 2009
124.
Organocatalysis—after the gold rush
Bertelsen S., Jørgensen K.A.
Chemical Society Reviews , 2009
125.
Berkessel A., Gröger H.
2005
126.
Organocatalysis by N-heterocyclic carbenes.
Enders D., Niemeier O., Henseler A.
Chemical Reviews , 2007
127.
Asymmetric organocatalysis
Pellissier H.
Tetrahedron , 2007
128.
Nucleophilic carbenes in asymmetric organocatalysis.
Enders D., Balensiefer T.
Accounts of Chemical Research , 2004
129.
In the golden age of organocatalysis.
Dalko P.I., Moisan L.
Angewandte Chemie - International Edition , 2004
130.
Evolution of asymmetric organocatalysis: multi- and retrocatalysis
131.
Low-loading asymmetric organocatalysis
Giacalone F., Gruttadauria M., Agrigento P., Noto R.
Chemical Society Reviews , 2012
132.
Applications of asymmetric organocatalysis in medicinal chemistry
Alemán J., Cabrera S.
Chemical Society Reviews , 2013
133.
133
C. Wilson
Trans. Electrochem. Soc. , 1941
135.
When Organocatalysis Meets Transition‐Metal Catalysis
Zhong C., Shi X.
European Journal of Organic Chemistry , 2010
137.
Mixtures of ionic liquids
Niedermeyer H., Hallett J.P., Villar-Garcia I.J., Hunt P.A., Welton T.
Chemical Society Reviews , 2012
139.
Recent advances in oxidation catalysis using ionic liquids as solvents
Betz D., Altmann P., Cokoja M., Herrmann W.A., Kühn F.E.
Coordination Chemistry Reviews , 2011
140.
Recent advances in ionic liquid catalysis
Zhang Q., Zhang S., Deng Y.
Green Chemistry , 2011
141.
141
Friedl.
142.
142
1913
143.
143
Friedl.
144.
Ionic liquids and deep eutectic solvents for biodiesel synthesis: a review
Zhao H., Baker G.A.
Journal of Chemical Technology and Biotechnology , 2012
145.
Transition Metal Nanoparticle Catalysis in Ionic Liquids
Scholten J.D., Leal B.C., Dupont J.
ACS Catalysis , 2011
146.
Recent advances of enzymatic reactions in ionic liquids
Moniruzzaman M., Nakashima K., Kamiya N., Goto M.
Biochemical Engineering Journal , 2010
150.
10.1002/1521-3773(20001103)39:21<3772::AID-ANIE3772>3.0.CO;2-5
151.
Applications of ionic liquids in the chemical industry
Plechkova N.V., Seddon K.R.
Chemical Society Reviews , 2008
152.
Catalysis in Ionic Liquids
Pârvulescu V.I., Hardacre C.
Chemical Reviews , 2007
153.
Synthesis and Application of Water-Soluble NHC Transition-Metal Complexes
Schaper L., Hock S.J., Herrmann W.A., Kühn F.E.
Angewandte Chemie - International Edition , 2012
155.
CH Bond Functionalization in Water Catalyzed by Carboxylato Ruthenium(II) Systems
Arockiam P., Fischmeister C., Bruneau C., Dixneuf P.
Angewandte Chemie - International Edition , 2010
156.
156
J. S. Fruton
J. Biol. Med. , 1950
157.
157
1903
158.
Organic Synthesis “On Water”
Chanda A., Fokin V.V.
Chemical Reviews , 2009
159.
159
J. Tafel
Z. Elektrochem. , 1911
160.
Stereoselective Organic Reactions in Water
Lindström U.M.
Chemical Reviews , 2002
161.
161
Friedl.
162.
162
1917
163.
Homogeneous catalysts based on water-soluble phosphines
164.
Reactions of C−H Bonds in Water
Herrerías C.I., Yao X., Li Z., Li C.
Chemical Reviews , 2007
167.
N-Heterocyclic carbene transition metal complexes for catalysis in aqueous media.
169.
Green chemistry oriented organic synthesis in water
Simon M., Li C.
Chemical Society Reviews , 2012
172.
Biocatalysis in Supercritical CO2
Matsuda T., Harada T., Nakamura K.
Current Organic Chemistry , 2005
173.
Heterogeneous Catalysis in Supercritical Media: 1. Carbon Dioxide
Kruse A., Vogel H.
Chemical Engineering and Technology , 2008
176.
176
G. V. Samsonov
"Metody Ispytaniya na Mikrotverdost' i Pribory" (Methods of Microhardness Testing and Apparatus) , 1965
178.
The Potential of Carbon Dioxide in Synthetic Organic Chemistry
Rayner C.M.
Organic Process Research and Development , 2006
179.
Homogeneous Catalysis in Supercritical Fluids
Jessop P.G., Ikariya T., Noyori R.
Chemical Reviews , 1999
180.
Solid-Phase Organic Synthesis in the Presence of Compressed Carbon Dioxide
Stobrawe A., Makarczyk P., Maillet C., Muller J., Leitner W.
Angewandte Chemie - International Edition , 2008
184.
PEG as an alternative reaction medium in metal-mediated transformations
Colacino E., Martinez J., Lamaty F., Patrikeeva L.S., Khemchyan L.L., Ananikov V.P., Beletskaya I.P.
Coordination Chemistry Reviews , 2012
185.
Solvent-Free Heterocyclic Synthesis
Martins M.A., Frizzo C.P., Moreira D.N., Buriol L., Machado P.
Chemical Reviews , 2009
186.
Green Chemistry: Principles and Practice
Anastas P., Eghbali N.
Chemical Society Reviews , 2010
189.
Advanced Liquid Chromatography−Mass Spectrometry Interface Based on Electron Ionization
Cappiello A., Famiglini G., Pierini E., Palma P., Trufelli H.
Analytical Chemistry , 2007
190.
Determination of Natural Pyrethrins by Liquid Chromatography-Electron Ionisation-Mass Spectrometry
Cappiello A., Tirillini B., Famiglini G., Trufelli H., Termopoli V., Flender C.
Phytochemical Analysis , 2011
191.
LC–MS with electron ionization of cold molecules in supersonic molecular beams
Granot O., Amirav A.
International Journal of Mass Spectrometry , 2005
193.
10.1002/1096-9888(200007)35:7<804::AID-JMS22>3.0.CO;2-Q
194.
Electrospray: From ions in solution to ions in the gas phase, what we know now
195.
Some Thoughts on Electrospray Ionization Mechanisms
Crotti S., Seraglia R., Traldi P.
European Journal of Mass Spectrometry , 2011
196.
Unraveling the Mechanism of Electrospray Ionization
Konermann L., Ahadi E., Rodriguez A.D., Vahidi S.
Analytical Chemistry , 2012
197.
Electrospray Wings for Molecular Elephants (Nobel Lecture)
Fenn J.B.
Angewandte Chemie - International Edition , 2003
199.
199
Yu. K. Delimarskii
Byull. Izobr. , 1970
201.
The Expanding Role of Electrospray Ionization Mass Spectrometry for Probing Reactive Intermediates in Solution
205.
Mass spectrometric screening of chiral catalysts and catalyst mixtures
Müller C.A., Markert C., Teichert A.M., Pfaltz A.
Chemical Communications , 2009
208.
Contribution to the Mechanism of Copper-Catalyzed C–N and C–O Bond Formation
Lefèvre G., Franc G., Tlili A., Adamo C., Taillefer M., Ciofini I., Jutand A.
Organometallics , 2012
209.
Belyakov Pavel Alekseevich, Kadentsev Valentin Ivanovich, Chizhov Alexander Olegovich, Kolotyrkina Natal'ya Georgievna, Shashkov Alexander Stepanovich, Ananikov Valentin Pavlovich
Mendeleev Communications , 2010
210.
Charged ligands for catalyst immobilisation and analysis
Chisholm D.M., Scott McIndoe J.
Dalton Transactions , 2008
211.
Probing Conformational Changes of Ubiquitin by Host–Guest Chemistry Using Electrospray Ionization Mass Spectrometry
Lee J.W., Heo S.W., Lee S.J., Ko J.Y., Kim H., Kim H.I.
Journal of the American Society for Mass Spectrometry , 2012
213.
Powerful Insight into Catalytic Mechanisms through Simultaneous Monitoring of Reactants, Products, and Intermediates
Vikse K.L., Ahmadi Z., Manning C.C., Harrington D.A., McIndoe J.S.
Angewandte Chemie - International Edition , 2011
214.
10.1002/1522-2675(20000906)83:9<2192::AID-HLCA2192>3.0.CO;2-G
215.
Mono-alkylated bisphosphines as dopants for ESI-MS analysis of catalytic reactions
Chisholm D.M., Oliver A.G., McIndoe J.S.
Dalton Transactions , 2010
217.
Pressurized sample infusion: An easily calibrated, low volume pumping system for ESI-MS analysis of reactions
Vikse K.L., Ahmadi Z., Luo J., van der Wal N., Daze K., Taylor N., McIndoe J.S.
International Journal of Mass Spectrometry , 2012
220.
Aerobic Dehydrogenative Heck Reactions of Heterocycles with Styrenes: A Negative Effect of Metallic Co-Oxidants
Vasseur A., Harakat D., Muzart J., Le Bras J.
Advanced Synthesis and Catalysis , 2012
223.
Determining the Enantioselectivity of Chiral Catalysts by Mass Spectrometric Screening of Their Racemic Forms
Ebner C., Müller C.A., Markert C., Pfaltz A.
Journal of the American Chemical Society , 2011
225.
Nanocluster Isotope Distributions Measured by Electrospray Time-of-Flight Mass Spectrometry
Comeau A.N., Liu J., Khadka C.B., Corrigan J.F., Konermann L.
Analytical Chemistry , 2012
226.
Tracking the Formation of a Polynuclear Co16 Complex and Its Elimination and Substitution Reactions by Mass Spectroscopy and Crystallography
227.
Unimolecular Reactivity of the [Urea-Sr]2+ Complex, a Metastable Dication in the Gas Phase: An Experimental and Theoretical Perspective
228.
The mechanisms of collisional activation of ions in mass spectrometry
231.
Controlled tin catalyzed hydrolysis of 3-acryloxypropyltrimethoxysilane with mono- and multi-functional mercaptans
Burkhalter R.S., Hogue C.L., Smith D.L., Sonner S.M., Winningham M.J., Youngman R.E.
Journal of Organometallic Chemistry , 2013
233.
Accelerated carbon-carbon bond-forming reactions in preparative electrospray.
Müller T., Badu-Tawiah A., Cooks R.G.
Angewandte Chemie - International Edition , 2012
236.
Microchip Atmospheric Pressure Chemical Ionization Source for Mass Spectrometry
Östman P., Marttila S.J., Kotiaho T., Franssila S., Kostiainen R.
Analytical Chemistry , 2004
237.
Effect of different solution flow rates on analyte ion signals in nano-ESI MS, or: when does ESI turn into nano-ESI?
Schmidt A., Karas M., Dülcks T.
Journal of the American Society for Mass Spectrometry , 2003
238.
Efficiency of nano-electrospray ionization
El-Faramawy A., Siu K.W., Thomson B.A.
Journal of the American Society for Mass Spectrometry , 2005
240.
240
W. A. Waters
"The Chemistry of Free Radicals" , 1948
241.
241
M. S. Kharasch
"Grignard Reactions of Nonmetallic Substances" , 1954
242.
Residual Dipolar Couplings (RDCs) in Organic Structure Determination
Thiele C.M.
European Journal of Organic Chemistry , 2008
244.
Structural Elucidation with NMR Spectroscopy: Practical Strategies for Organic Chemists
247.
247
E. I. Levkoeva
Khim. Geterotsikl. Soed. , 1976
248.
248
M. Ya. Fioshin
Plasticheskie Massy , 1960
249.
249
A. I. Fedorova
Dokl. Akad. Nauk SSSR , 1961
250.
250
D. Goerrig
1955
251.
QQ-HSQC: a quick, quantitative heteronuclear correlation experiment for NMR spectroscopy
Peterson D.J., Loening N.M.
Magnetic Resonance in Chemistry , 2007
252.
The conformations of 17β-estradiol (E2) and 17α-estradiol as determined by solution NMR
Guo J., Duclos R.I., Vemuri V.K., Makriyannis A.
Tetrahedron Letters , 2010
254.
3- and 19-Oximes of 16α,17α-cyclohexanoprogesterone derivatives: Synthesis and interactions with progesterone receptor and other proteins
257.
13C-{1H,11B} triple-resonance experiments. Sign determination of 1J(11B-11B), J(13C-11B), and 2J(1H-11B) in some organoboron compounds
Zozulin A.J., Jakobsen H.J., Moore T.F., Garber A.R., Odom J.D.
Journal of Magnetic Resonance (1969) , 1980
258.
Applications of 19F multidimensional NMR
BATTISTE J., NEWMARK R.
Progress in Nuclear Magnetic Resonance Spectroscopy , 2006
259.
Determination of size and sign of hetero-nuclear coupling constants from 2D 19F–13C correlation spectra
Ampt K.A., Aspers R.L., Dvortsak P., van der Werf R.M., Wijmenga S.S., Jaeger M.
Journal of Magnetic Resonance , 2012
260.
Transformation of homonuclear two-dimensional NMR techniques into one-dimensional techniques using Gaussian pulses
Kessler H., Oschkinat H., Griesinger C., Bermel W.
Journal of Magnetic Resonance (1969) , 1986
261.
Excitation Sculpting in High-Resolution Nuclear Magnetic Resonance Spectroscopy: Application to Selective NOE Experiments
Stott K., Stonehouse J., Keeler J., Hwang T., Shaka A.J.
Journal of the American Chemical Society , 1995
262.
Ultrahigh-Quality NOE Spectra
Stonehouse J., Adell P., Keeler J., Shaka A.J.
Journal of the American Chemical Society , 1994
263.
MLEV-17-based two-dimensional homonuclear magnetization transfer spectroscopy
266.
266
N. G. Mudrik
1975
267.
Synthesis, NMR and Conformational Studies of Fucoidan Fragments. V.[1] Linear 4,4′,4″‐Tri‐O‐Sulfated and Parent Non‐sulfated (1→3)‐Fucotrioside Fragments
Gerbst A.G., Ustuzhanina N.E., Grachev A.A., Khatuntseva E.A., Tsvetkov D.E., Shashkov A.S., Usov A.I., Preobrazhenskaya M.E., Ushakova N.A., Nifantiev N.E.
Journal of Carbohydrate Chemistry , 2003
268.
Concentration Measurement by Proton NMR Using the ERETIC Method
Akoka S., Barantin L., Trierweiler M.
Analytical Chemistry , 1999
269.
Principles and Features of Single-Scan Two-Dimensional NMR Spectroscopy
Frydman L., Lupulescu A., Scherf T.
Journal of the American Chemical Society , 2003
270.
Single-Scan NMR Spectroscopy at Arbitrary Dimensions
Shrot Y., Frydman L.
Journal of the American Chemical Society , 2003
271.
A new detection scheme for ultrafast 2D J-resolved spectroscopy
Giraudeau P., Akoka S.
Journal of Magnetic Resonance , 2007
272.
Ultrafast Quantitative 2D NMR: An Efficient Tool for the Measurement of Specific Isotopic Enrichments in Complex Biological Mixtures
Giraudeau P., Massou S., Robin Y., Cahoreau E., Portais J., Akoka S.
Analytical Chemistry , 2011
273.
Real-time multidimensional NMR follows RNA folding with second resolution
Lee M., Gal M., Frydman L., Varani G.
Proceedings of the National Academy of Sciences of the United States of America , 2010
274.
Monitoring Mechanistic Details in the Synthesis of Pyrimidines via Real-Time, Ultrafast Multidimensional NMR Spectroscopy
Pardo Z.D., Olsen G.L., Fernández-Valle M.E., Frydman L., Martínez-Álvarez R., Herrera A.
Journal of the American Chemical Society , 2012
275.
Multiple Ultrafast, Broadband 2D NMR Spectra of Hyperpolarized Natural Products
Giraudeau P., Shrot Y., Frydman L.
Journal of the American Chemical Society , 2009
278.
Self-diffusion in polymer systems studied by magnetic field-gradient spin-echo NMR methods
Walderhaug H., Söderman O., Topgaard D.
Progress in Nuclear Magnetic Resonance Spectroscopy , 2010
279.
10.1002/(SICI)1099-0534(1997)9:5<299::AID-CMR2>3.0.CO;2-U
281.
Two distinct mechanisms of alkyne insertion into the metal-sulfur bond: Combined experimental and theoretical study and application in catalysis
Ananikov V., Gayduk K., Orlov N., Beletskaya I., Khrustalev V., Antipin M.
Chemistry - A European Journal , 2010
283.
Toward the ideal catalyst: From atomic centers to a "cocktail" of catalysts
284.
Pure Shift 1H NMR: A Resolution of the Resolution Problem?
Aguilar J., Faulkner S., Nilsson M., Morris G.
Angewandte Chemie - International Edition , 2010
285.
A homodecoupled diffusion experiment for the analysis of complex mixtures by NMR
Cobas J.C., Martín-Pastor M.
Journal of Magnetic Resonance , 2004
286.
An Improved Diffusion-Ordered Spectroscopy Experiment Incorporating Bipolar-Gradient Pulses
Wu D.H., Chen A.D., Johnson C.S.
Journal of Magnetic Resonance Series A , 1995
287.
High resolution 13C DOSY: The DEPTSE experiment
Botana A., Howe P.W., Caër V., Morris G.A., Nilsson M.
Journal of Magnetic Resonance , 2011
289.
Difftrain: A Novel Approach to a True Spectroscopic Single-Scan Diffusion Measurement
Stamps J.P., Ottink B., Visser J.M., van Duynhoven J.P., Hulst R.
Journal of Magnetic Resonance , 2001
290.
290
Guntz
Compt. rend. , 1902
292.
Flow techniques in NMR spectroscopy
Keifer P.A.
Annual Reports on NMR Spectroscopy , 2007
293.
Testosterone 1β-hydroxylation by human cytochrome P450 3A4
Krauser J.A., Voehler M., Tseng L., Schefer A.B., Godejohann M., Guengerich F.P.
FEBS Journal , 2004
294.
Targeted Acquisition for Real-Time NMR Spectroscopy
Jaravine V.A., Orekhov V.Y.
Journal of the American Chemical Society , 2006
295.
Analysis of non-uniformly sampled spectra with multi-dimensional decomposition
Orekhov V.Y., Jaravine V.A.
Progress in Nuclear Magnetic Resonance Spectroscopy , 2011
296.
Double-quantum biased covariance spectroscopy: Application to the 2D INADEQUATE experiment
Zhang F., Trbovic N., Wang J., Brüschweiler R.
Journal of Magnetic Resonance , 2005
297.
A Covariance NMR Toolbox for MATLAB and OCTAVE
Short T., Alzapiedi L., Brüschweiler R., Snyder D.
Journal of Magnetic Resonance , 2011
301.
Mechanochemistry: opportunities for new and cleaner synthesis
James S.L., Adams C.J., Bolm C., Braga D., Collier P., Friščić T., Grepioni F., Harris K.D., Hyett G., Jones W., Krebs A., Mack J., Maini L., Orpen A.G., Parkin I.P., et. al.
Chemical Society Reviews , 2012
303.
Ball milling in organic synthesis: solutions and challenges
Stolle A., Szuppa T., Leonhardt S.E., Ondruschka B.
Chemical Society Reviews , 2011
304.
Chemoselective, solvent-free aldol condensation reaction
Raston C.L., Scott J.L.
Green Chemistry , 2000
305.
A Highly Efficient Asymmetric Organocatalytic Aldol Reaction in a Ball Mill
Rodríguez B., Bruckmann A., Bolm C.
Chemistry - A European Journal , 2007
307.
Reformatsky and Luche reaction in the absence of solvent
Tanaka K., Kishigami S., Toda F.
Journal of Organic Chemistry , 1991
308.
A simplified green chemistry approach to the Biginelli reaction using ‘Grindstone Chemistry’
Bose A.K., Pednekar S., Ganguly S.N., Chakraborty G., Manhas M.S.
Tetrahedron Letters , 2004
311.
Mechanically Induced Solid-State Generation of Phosphorus Ylides and the Solvent-Free Wittig Reaction
Balema V.P., Wiench J.W., Pruski M., Pecharsky V.K.
Journal of the American Chemical Society , 2002
313.
Mechanically activated synthesis of 1,3,5-triaryl-2-pyrazolines by high speed ball milling
317.
Solid-state and solvent-free synthesis of azines, pyrazoles, and pyridazinones using solid hydrazine
Lee B., Kang P., Lee K.H., Cho J., Nam W., Lee W.K., Hur N.H.
Tetrahedron Letters , 2013
318.
Solvent-Free Synthesis of Peptides
Declerck V., Nun P., Martinez J., Lamaty F.
Angewandte Chemie - International Edition , 2009
319.
Green Synthesis of α,β- and β,β-Dipeptides under Solvent-Free Conditions
Hernández J.G., Juaristi E.
Journal of Organic Chemistry , 2010
320.
Solvent-free synthesis of metal complexes
Garay A.L., Pichon A., James S.L.
Chemical Society Reviews , 2007
321.
The first solid phase synthesis of pincer palladium complexes
Kozlov V.A., Aleksanyan D.V., Korobov M.V., Avramenko N.V., Aysin R.R., Maloshitskaya O.A., Korlyukov A.S., Odinets I.L.
Dalton Transactions , 2011
323.
The Heck reaction under ball-milling conditions
Tullberg E., Peters D., Frejd T.
Journal of Organometallic Chemistry , 2004
324.
Fast copper-, ligand- and solvent-free Sonogashira coupling in a ball mill
Thorwirth R., Stolle A., Ondruschka B.
Green Chemistry , 2010
325.
Suzuki cross-couplings of (hetero)aryl chlorides in the solid-state
Cravotto G., Garella D., Tagliapietra S., Stolle A., Schüßler S., Leonhardt S.E., Ondruschka B.
New Journal of Chemistry , 2012
326.
Fast, Ligand- and Solvent-Free Synthesis of 1,4-Substituted Buta-1,3-diynes by Cu-Catalyzed Homocoupling of Terminal Alkynes in a Ball Mill
Schmidt R., Thorwirth R., Szuppa T., Stolle A., Ondruschka B., Hopf H.
Chemistry - A European Journal , 2011
327.
Solvent-Free Asymmetric Organocatalysis in a Ball Mill
Rodríguez B., Rantanen T., Bolm C.
Angewandte Chemie - International Edition , 2006
329.
Solvent-Free Asymmetric Anhydride Opening in a Ball Mill
Rantanen T., Schiffers I., Bolm C.
Organic Process Research and Development , 2007
332.
Solvent-free Sonogashira coupling reaction via high speed ball milling
Fulmer D.A., Shearouse W.C., Medonza S.T., Mack J.
Green Chemistry , 2009
333.
Crystal engineering of topochemical solid state reactions
Biradha K., Santra R.
Chemical Society Reviews , 2013
335.
335
A. C. Byrns
1967
338.
Template‐Controlled Reactivity in the Organic Solid State by Principles of Coordination‐Driven Self‐Assembly
Bučar D., Papaefstathiou G.S., Hamilton T.D., Chu Q.L., Georgiev I.G., MacGillivray L.R.
European Journal of Inorganic Chemistry , 2007
341.
Real-time and in situ monitoring of mechanochemical milling reactions
Friščić T., Halasz I., Beldon P.J., Belenguer A.M., Adams F., Kimber S.A., Honkimäki V., Dinnebier R.E.
Nature Chemistry , 2012
342.
How grinding evolves
Harris K.D.
Nature Chemistry , 2012
343.
13C NMR investigation of carbon nanotubes and derivatives
Goze Bac C., Bernier P., Latil S., Jourdain V., Rubio A., Jhang S.H., Lee S.W., Park Y.W., Holzinger M., Hirsch A.
Current Applied Physics , 2001
345.
High-Resolution Solid-State NMR Spectroscopy of Steroids and Their Derivatives
346.
Synthesis and characterisation of uranyl substituted malonato complexes
Zhang Y., Collison D., Livens F.R., Helliwell M., Heatley F., Powell A.K., Wocadlo S., Eccles H.
Polyhedron , 2002
347.
Applications of high-resolution 1H solid-state NMR
Brown S.P.
Solid State Nuclear Magnetic Resonance , 2012
348.
Electron-nuclear cross polarization
Weis V., Griffin R.G.
Solid State Nuclear Magnetic Resonance , 2006
349.
Surface enhanced NMR spectroscopy by dynamic nuclear polarization.
Lesage A., Lelli M., Gajan D., Caporini M.A., Vitzthum V., Miéville P., Alauzun J., Roussey A., Thieuleux C., Mehdi A., Bodenhausen G., Coperet C., Emsley L.
Journal of the American Chemical Society , 2010
350.
Catalytic adaptive recognition of thiol (SH) and selenol (SeH) groups toward synthesis of functionalized vinyl monomers
Ananikov V.P., Orlov N.V., Zalesskiy S.S., Beletskaya I.P., Khrustalev V.N., Morokuma K., Musaev D.G.
Journal of the American Chemical Society , 2012
353.
Heterogeneous Catalysis by Gold
Takei T., Akita T., Nakamura I., Fujitani T., Okumura M., Okazaki K., Huang J., Ishida T., Haruta M.
Advances in Catalysis , 2012
355.
Recent developments and applications of electron microscopy to heterogeneous catalysis
Yang J.C., Small M.W., Grieshaber R.V., Nuzzo R.G.
Chemical Society Reviews , 2012
360.
360
J. Wlodyka
Rudy i Metale niezel. , 1970
361.
Single Crystalline Submicrotubes from Small Organic Molecules
Zhao Y.S., Yang W., Xiao D., Sheng X., Yang X., Shuai Z., Luo Y., Yao J.
Chemistry of Materials , 2005