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Derivatization in gas chromatographic determination of phenol and aniline traces in aqueous media

Ivan Vladimirovich Gruzdev ¹

Ivan Vladimirovich Gruzdev

Igor' Georgievich Zenkevich ²

Igor' Georgievich Zenkevich

Boris Mikhailovich Kondratenok ¹

Boris Mikhailovich Kondratenok

¹ Institute of Biology, Komi Scientific Center of Ural Branch of RAS, Syktyvkar

² Institute of Chemistry, St. Petersburg State University

10.1070/RCR4553

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Published 30 November 2014

Communication , Volume 84, Issue 6, 653-664

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2015, Volume 84, Issue 6

1 June 2015

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Gruzdev I. V., Zenkevich I. G., Kondratenok B. M. Derivatization in gas chromatographic determination of phenol and aniline traces in aqueous media // Russian Chemical Reviews. 2015. Vol. 84. No. 6. pp. 653-664.

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TY - JOUR

DO - 10.1070/RCR4553

UR - https://rcr.colab.ws/publications/10.1070/RCR4553

TI - Derivatization in gas chromatographic determination of phenol and aniline traces in aqueous media

T2 - Russian Chemical Reviews

AU - Gruzdev, Ivan Vladimirovich

AU - Zenkevich, Igor' Georgievich

AU - Kondratenok, Boris Mikhailovich

PY - 2015

DA - 2014/11/30

PB - ANO Editorial Board of the journal Uspekhi Khimii

SP - 653-664

IS - 6

VL - 84

ER -

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@article{2015_Gruzdev,

author = {Ivan Vladimirovich Gruzdev and Igor' Georgievich Zenkevich and Boris Mikhailovich Kondratenok},

title = {Derivatization in gas chromatographic determination of phenol and aniline traces in aqueous media},

journal = {Russian Chemical Reviews},

year = {2015},

volume = {84},

publisher = {ANO Editorial Board of the journal Uspekhi Khimii},

month = {Nov},

url = {https://rcr.colab.ws/publications/10.1070/RCR4553},

number = {6},

pages = {653--664},

doi = {10.1070/RCR4553}

}

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Gruzdev, Ivan Vladimirovich, et al. “Derivatization in gas chromatographic determination of phenol and aniline traces in aqueous media.” Russian Chemical Reviews, vol. 84, no. 6, Nov. 2015, pp. 653-664. https://rcr.colab.ws/publications/10.1070/RCR4553.

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Abstract

Substituted anilines and phenols are the most common hydrophilic organic environmental toxicants. The principles of gas chromatographic determination of trace amounts of these compounds in aqueous media at concentrations $\le0.1\ \mu$g\,litre$^{-1}$ based on synthesis of their derivatives (derivatization) directly in the aqueous phase are considered. Conversion of relatively hydrophilic analytes into more hydrophobic derivatives makes it possible to achieve such low detection limits and optimize the protocols of extractive preconcentration and selective chromatographic detection. Among the known reactions, this condition is best met by electrophilic halogenation of compounds at the aromatic moiety.

The bibliography includes 177 references.

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